Issue 10, 1986

Studies of reactions of 1,3,5-trimethylbiuret and 1,3-dimethylurea with chloroform

Abstract

1,3,5-Trimethylbiuret and 1,3-dimethylurea react with chloroform at temperatures above 200 °C to produce 1,3,5-trimethyl-1,3,5-triazinane-2,4-dione (4), 1,3-dimethyl-1,3,5-triazinane-2,4,6-trione (5), and 1,3,5-trimethyl-1,3,5-triazinane-2,4,6-trione [methyl isocyanate (MIC) trimer](3), besides minor quantities of other by-products, via trimerization reactions involving MIC, isocyanic acid, and N- methylenemethylamine.

Article information

Article type
Paper

J. Chem. Soc., Chem. Commun., 1986, 795-796

Studies of reactions of 1,3,5-trimethylbiuret and 1,3-dimethylurea with chloroform

T. D. J. D'Silva and A. Lopes, J. Chem. Soc., Chem. Commun., 1986, 795 DOI: 10.1039/C39860000795

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