Issue 10, 2008
From the journal:

Organic & Biomolecular Chemistry

An efficient method for synthesising unsymmetrical silaketals: substrates for ring-closing, including macrocycle-closing, metathesis†

Christopher Cordier,ab   Daniel Morton,ab   Stuart Leach,ab   Thomas Woodhall,ab   Catherine O'Leary-Steele,ab   Stuart Warrinerab  and  Adam Nelson*ab  

* Corresponding authors

a School of Chemistry, University of Leeds, Leeds, UK
E-mail: a.s.nelson@leeds.ac.uk
Fax: +44 (0)113 343 6565
Tel: +44 (0)113 343 6502

b Astbury Centre for Structural Molecular Biology, University of Leeds, Leeds, UK

Abstract

Diisopropylsilyl ethers were activated with N-bromosuccinimide, and reacted with a fluorous-tagged alcohol, to yield tethered substrates for ring-closing metathesis reactions.

Graphical abstract: An efficient method for synthesising unsymmetrical silaketals: substrates for ring-closing, including macrocycle-closing, metathesis

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Article information

DOI
https://doi.org/10.1039/B804769N
Article type
Communication
Submitted
19 Mar 2008
Accepted
20 Mar 2008
First published
10 Apr 2008
This article is Open Access

Org. Biomol. Chem., 2008,6, 1734-1737

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An efficient method for synthesising unsymmetrical silaketals: substrates for ring-closing, including macrocycle-closing, metathesis

C. Cordier, D. Morton, S. Leach, T. Woodhall, C. O'Leary-Steele, S. Warriner and A. Nelson, Org. Biomol. Chem., 2008, 6, 1734 DOI: 10.1039/B804769N

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