Issue 29, 2011

Synthesis and structure of all-syn-1,2,3,4-tetrafluorocyclohexane

Abstract

Preparation of the all-syn isomer of 1,2,3,4-tetrafluorocyclohexane is reported; X-ray structural studies shows a conformation with two of the C–F bonds oriented 1,3-diaxial to each other and 19F-NMR reveals a through space diaxial 4JFF coupling constant of 29 Hz.

Graphical abstract: Synthesis and structure of all-syn-1,2,3,4-tetrafluorocyclohexane

Supplementary files

Article information

Article type
Communication
Submitted
23 May 2011
Accepted
14 Jun 2011
First published
28 Jun 2011

Chem. Commun., 2011,47, 8265-8267

Synthesis and structure of all-syn-1,2,3,4-tetrafluorocyclohexane

A. J. Durie, A. M. Z. Slawin, T. Lebl, P. Kirsch and D. O'Hagan, Chem. Commun., 2011, 47, 8265 DOI: 10.1039/C1CC13016A

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