One-minute synthesis of crystalline microporous aluminophosphate (AlPO4-5) by combining fast heating with a seed-assisted method

Zhendong Liu; Toru Wakihara; Daisuke Nishioka; Kazunori Oshima; Takahiko Takewaki; Tatsuya Okubo

doi:10.1039/C3CC49548E

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One-minute synthesis of crystalline microporous aluminophosphate (AlPO₄-5) by combining fast heating with a seed-assisted method†

Zhendong Liu,^a Toru Wakihara,^a Daisuke Nishioka,^b Kazunori Oshima,^b Takahiko Takewaki^b and Tatsuya Okubo*^a

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* Corresponding authors

^a Department of Chemical System Engineering, The University of Tokyo, 7-3-1 Hongo, Bunkyo-ku, Tokyo 113-8656, Japan
E-mail: okubo@chemsys.t.u-tokyo.ac.jp
Fax: +81-3-5800-3806
Tel: +81-3-5841-7348

^b Mitsubishi Chemical Group, Science and Technology Research Center, 1000 Kamoshida-cho, Aoba-ku, Yokohama 227-8502, Japan

Abstract

Herein, we report a rapid route for the synthesis of AlPO₄-5. By combining fast heating in a tubular reactor with a seed-assisted method, both of which were found to be crucial, the preparation of AlPO₄-5 was completed in one minute, making this route the fastest known for the preparation of the crystalline microporous materials.

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Article information

DOI: https://doi.org/10.1039/C3CC49548E
Article type: Communication
Submitted: 17 Dec 2013
Accepted: 10 Jan 2014
First published: 10 Jan 2014

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Chem. Commun., 2014,50, 2526-2528

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One-minute synthesis of crystalline microporous aluminophosphate (AlPO₄-5) by combining fast heating with a seed-assisted method

Z. Liu, T. Wakihara, D. Nishioka, K. Oshima, T. Takewaki and T. Okubo, Chem. Commun., 2014, 50, 2526 DOI: 10.1039/C3CC49548E

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Chemical Communications