Novel phosphonium salts of diacetoxyiodine(I) anions 1 add to alkenes like tri-O-benzyl galactal 8 affording 1-acetoxy-2-iodopyranoses 12a,b which can efficiently be employed in the synthesis of 2-deoxyglycoside 14.
A. Kirschning, C. Plumeier and L. Rose, Chem. Commun., 1998, 33 DOI: 10.1039/A706305I
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