Ozone has been used to remove the organic surfactant species at 250 °C from as synthesised organic/inorganic composite (or mesophase) materials to form mesoporous MCM-41 type solids with higher surface area, larger pores and narrower pore size distribution than those obtained by conventional calcination at 550 °C.
M. T. J. Keene, R. Denoyel and P. L. Llewellyn, Chem. Commun., 1998, 2203 DOI: 10.1039/A806118A
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