Issue 20, 1999
From the journal:

Chemical Communications

An unpaired electron incarcerated within an icosahedral borane cage: synthesis and crystal structure of the blue, air-stable {[closo-B12(CH3)12]·}– radical

Toralf Peymann,   Carolyn B. Knobler  and  M. Frederick Hawthorne  

Abstract

Oxidation of the permethylated icosahedral borane [closo-B12(CH3)12]2– 1, by ceric(IV) ammonium nitrate in acetonitrile affords the blue, air-stable paramagnetic anion {[closo-B12(CH3)12]·}– 2, which has been characterized, among other means, by X-ray crystallography.

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DOI
https://doi.org/10.1039/A905406E
Article type
Paper

Chem. Commun., 1999, 2039-2040

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An unpaired electron incarcerated within an icosahedral borane cage: synthesis and crystal structure of the blue, air-stable {[closo-B12(CH3)12]·}– radical

T. Peymann, C. B. Knobler and M. Frederick Hawthorne, Chem. Commun., 1999, 2039 DOI: 10.1039/A905406E

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