Issue 7, 2000
From the journal:

Chemical Communications

Synthesis and spectroscopic characterisation of all the intermediates in the Pd-catalysed methoxycarbonylation of ethene

Graham R. Eastham,a   Brian T. Heaton,*b   Jonathan A. Iggo,b   Robert P. Tooze,a   Robin Whymanb  and  Stefano Zacchinib  

* Corresponding authors

a Ineos Acrylics, PO Box 90, Wilton, Cleveland, Middlesborough, UK

b Chemistry Department, University of Liverpool, Liverpool, UK
E-mail: amf@liv.ac.uk

Abstract

The pathway of the palladium catalysed methoxycarbonylation of ethene to methyl propanoate has been shown to occur via a hydride rather than a methoxycarbonyl cycle and all the intermediates in this cycle have been unambiguously identified by multinuclear NMR spectroscopy and 13C-labelling.

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Article information

DOI
https://doi.org/10.1039/B001110J
Article type
Communication
Submitted
14 Jan 2000
Accepted
28 Feb 2000
First published
22 Mar 2000

Chem. Commun., 2000, 609-610

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Synthesis and spectroscopic characterisation of all the intermediates in the Pd-catalysed methoxycarbonylation of ethene

G. R. Eastham, B. T. Heaton, J. A. Iggo, R. P. Tooze, R. Whyman and S. Zacchini, Chem. Commun., 2000, 609 DOI: 10.1039/B001110J

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