SCHEDULED MAINTENANCE
Protection of aldehydes and ketones as hemithioacetals or dithioacetals by an exchange reaction from 2,2-dimethyl-1,3-oxathiolane or 2,2-dimethyl-1,3-dithiolane catalyzed by solid acidic catalysts is readily achieved without solvent under microwave irradiation.
Oxathiolane and dithiolane exchange reaction for carbonyl group protection: a new, fast and efficient procedure without solvent under microwave irradiation
B. Pério and J. Hamelin, Green Chem., 2000, 2, 252 DOI: 10.1039/B005937O
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