Issue 10, 2003
From the journal:

Journal of Materials Chemistry

Microwave-assisted synthesis of nanosized MoSe2

Riki Harpeness,a   Aharon Gedanken,*a   A. M. Weissb  and  M. A. Slifkinb  

* Corresponding authors

a Department of Chemistry, Bar-Ilan University, Ramat-Gan, Israel
E-mail: gedanken@mail.biu.ac.il
Fax: +972-3-5351250
Tel: +972-3-5318315

b Department of Electronics, Jerusalem College of Technology, Jerusalem, Israel

Abstract

A microwave-assisted reaction between Mo(CO)6 and Se has yielded MoSe2 nanoparticles. Nanorods of MoSe2 of lengths ranging from 45 to 55 nanometers are identified in the product mixture. The prepared MoSe2 has been characterized by X-ray powder diffraction measurements, FTIR spectroscopy, photoacoustic spectroscopy (PAS), transmission electron microscopy (TEM) and high resolution TEM (HRTEM).

Graphical abstract: Microwave-assisted synthesis of nanosized MoSe2

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Article information

DOI
https://doi.org/10.1039/B303740A
Article type
Paper
Submitted
04 Apr 2003
Accepted
14 Aug 2003
First published
27 Aug 2003

J. Mater. Chem., 2003,13, 2603-2606

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Microwave-assisted synthesis of nanosized MoSe2

R. Harpeness, A. Gedanken, A. M. Weiss and M. A. Slifkin, J. Mater. Chem., 2003, 13, 2603 DOI: 10.1039/B303740A

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