Issue 22, 2003
From the journal:

Physical Chemistry Chemical Physics

Using a novel plug flow reactor for the in situ, simultaneous, monitoring of SAXS and WAXD during crystallisation from solution

Harvey G. Alison,a   Roger J. Davey,*a   John Garside,a   Michael J. Quayle,a   Gordon J. T. Tiddy,a   David T. Clarkeb  and  Gareth R. Jonesb  

* Corresponding authors

a Molecular Materials Centre, Department of Chemical Engineering, UMIST, P. O. Box 88, Manchester, UK
E-mail: r.j.davey@umist.ac.uk
Fax: +44 (0) 161 200 4399
Tel: +44 (0) 161 200 4409

b Daresbury Laboratory, Daresbury, Warrington, Cheshire, UK

Abstract

The design and application of a novel plug flow crystalliser is described. Simultaneous collection of SAXS and WAXD during the nucleation and crystal growth of a small organic molecule from solution is reported. Preliminary data imply the separation of a non-diffracting phase prior to the appearance of crystalline solid.

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Article information

DOI
https://doi.org/10.1039/B309309C
Article type
Communication
Submitted
04 Aug 2003
Accepted
03 Oct 2003
First published
14 Oct 2003

Phys. Chem. Chem. Phys., 2003,5, 4998-5000

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Using a novel plug flow reactor for the in situ, simultaneous, monitoring of SAXS and WAXD during crystallisation from solution

H. G. Alison, R. J. Davey, J. Garside, M. J. Quayle, G. J. T. Tiddy, D. T. Clarke and G. R. Jones, Phys. Chem. Chem. Phys., 2003, 5, 4998 DOI: 10.1039/B309309C

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