Formation of a new (1T) trigonal NbS2 polytype via atmospheric pressure chemical vapour deposition

Claire J. Carmalt; Troy D. Manning; Ivan P. Parkin; Emily S. Peters; Andrew L. Hector

doi:10.1039/B315782M

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Formation of a new (1T) trigonal NbS₂ polytype via atmospheric pressure chemical vapour deposition†

Claire J. Carmalt,*^a Troy D. Manning,^a Ivan P. Parkin,^a Emily S. Peters^a and Andrew L. Hector^b

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* Corresponding authors

^a Department of Chemistry, University College London, 20 Gordon Street, London, UK
E-mail: c.j.carmalt@ucl.ac.uk
Fax: 44 207 679 7463
Tel: 44 207 679 7528

^b School of Chemistry, University of Southampton, Highfield, Southampton, UK
Fax: 44 23 8059 6805
Tel: 44 23 8059 4125

Abstract

The formation of a new trigonal polytype of niobium disulfide, 1T-NbS₂, is described from the atmospheric pressure chemical vapour deposition reaction of niobium pentachloride with hexamethyldisilathiane and tert-butyl disulfide at 400–600 °C; films were grown on glass and those deposited at 500–600 °C were crystalline.

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Article information

DOI: https://doi.org/10.1039/B315782M
Article type: Communication
Submitted: 03 Dec 2003
Accepted: 10 Dec 2003
First published: 23 Dec 2003

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J. Mater. Chem., 2004,14, 290-291

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Formation of a new (1T) trigonal NbS₂ polytype via atmospheric pressure chemical vapour deposition

C. J. Carmalt, T. D. Manning, I. P. Parkin, E. S. Peters and A. L. Hector, J. Mater. Chem., 2004, 14, 290 DOI: 10.1039/B315782M

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Journal of Materials Chemistry