Issue 32, 2006
From the journal:

Chemical Communications

A new 17O-isotopic enrichment method for the NMR characterisation of phosphate compounds

Alexandrine Flambard,a   Lionel Montagne*a  and  Laurent Delevoyea  

* Corresponding authors

a UCCS, Unité de Catalyse et Chimie du Solide, UMR-CNRS 8181, Ecole Nationale Supérieure de Chimie de Lille, Université des Sciences et Technologies de Lille, BP90108, France
E-mail: lionel.montagne@univ-lille1.fr

Abstract

Heating phosphate compounds under 17O-enriched water vapour is an easy and rapid method to prepare homogeneously enriched and pure samples for the acquisition of 17O NMR spectra with a good sensitivity.

Graphical abstract: A new 17O-isotopic enrichment method for the NMR characterisation of phosphate compounds

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Article information

DOI
https://doi.org/10.1039/B604803J
Article type
Communication
Submitted
04 Apr 2006
Accepted
23 Jun 2006
First published
06 Jul 2006

Chem. Commun., 2006, 3426-3428

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A new 17O-isotopic enrichment method for the NMR characterisation of phosphate compounds

A. Flambard, L. Montagne and L. Delevoye, Chem. Commun., 2006, 3426 DOI: 10.1039/B604803J

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