Issue 10, 2007
From the journal:

CrystEngComm

Solvent effect in a “solvent free” reaction†

Dario Braga,*a   Stefano Luca Giaffreda,b   Fabrizia Grepioni,a   Michele R. Chierotti,c   Roberto Gobetto,*c   Giuseppe Palladinoa  and  Marco Politoa  

* Corresponding authors

a Dipartimento di Chimica G. Ciamician, Università di Bologna, Via F. Selmi 2, Bologna, Italy
E-mail: dario.braga@unibo.it
Fax: (39)051-2099456

b PolyCrystalLine s.r.l., Via Stradelli Guelfi 40/c, Bologna, Italy

c Dipartimento di Chimica I.F.M. Università di Torino, Via P. Giuria 7, Torino, Italy
E-mail: roberto.gobetto@unito.it
Fax: (39)011-6707855

Abstract

Vapour digestion of a mixture of solid [Fe(η5-C5H4–C5H4N)2] and solid pimelic acid HOOC(CH2)5COOH in the presence of solvent vapours generates co-crystals of different stoichiometry depending on the protic or aprotic nature of the solvent. The nature of the products has been ascertained by a combined use of SSNMR and X-ray diffraction.

Graphical abstract: Solvent effect in a “solvent free” reaction

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Article information

DOI
https://doi.org/10.1039/B711983F
Article type
Communication
Submitted
03 Aug 2007
Accepted
03 Aug 2007
First published
20 Aug 2007

CrystEngComm, 2007,9, 879-881

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Solvent effect in a “solvent free” reaction

D. Braga, S. L. Giaffreda, F. Grepioni, M. R. Chierotti, R. Gobetto, G. Palladino and M. Polito, CrystEngComm, 2007, 9, 879 DOI: 10.1039/B711983F

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