Issue 40, 2008
From the journal:

Chemical Communications

Single-crystal to single-crystal phase transition of cucurbit[5]uril hydrochloridehydrates: large water-filled channels transforming to layers of unusual stability†

David Bardelang,*a   Konstantin A. Udachin,a   Roberto Anedda,b   Igor Moudrakovski,a   Donald M. Leek,a   John A. Ripmeester*a  and  Christopher I. Ratcliffea  

* Corresponding authors

a NRC Steacie Institute for Molecular Sciences, 100 Sussex Dr., Ottawa, Canada
E-mail: david.bardelang@nrc-cnrc.gc.ca
Fax: +1 613 998 7833
Tel: +1 613 993 7694

b Porto Conte Ricerche Srl, S.P. 55 Porto Conte/Capo CacciaKm 8.400 Loc. Tramariglio, Alghero (SS), Italy

Abstract

Cucurbit[5]uril hydrochloride hydrate crystals with large water-filled channels transform to a highly stable layer structure via a single-crystal to single-crystal mechanism; 129Xe NMR showed that porosity in CB[5] samples depends critically on the method of preparation.

Graphical abstract: Single-crystal to single-crystal phase transition of cucurbit[5]uril hydrochloride hydrates: large water-filled channels transforming to layers of unusual stability

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Article information

DOI
https://doi.org/10.1039/B807033D
Article type
Communication
Submitted
06 May 2008
Accepted
08 Jun 2008
First published
27 Aug 2008

Chem. Commun., 2008, 4927-4929

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Single-crystal to single-crystal phase transition of cucurbit[5]uril hydrochloride hydrates: large water-filled channels transforming to layers of unusual stability

D. Bardelang, K. A. Udachin, R. Anedda, I. Moudrakovski, D. M. Leek, J. A. Ripmeester and C. I. Ratcliffe, Chem. Commun., 2008, 4927 DOI: 10.1039/B807033D

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