Issue 1, 2011
From the journal:

CrystEngComm

Novel form V of tolbutamide and a high Z′ crystal structure of form III†

Naba K. Natha  and  Ashwini Nangia*a  

* Corresponding authors

a School of Chemistry, University of Hyderabad, Prof. C. R. Rao Road, Gachibowli, Central University PO, Hyderabad, India
E-mail: ashwini.nangia@gmail.com

Abstract

Attempted co-crystallization of tolbutamide with p-phenylenediboronic acid and p-nitrophenol in EtOH afforded a modulated high Z′ crystal structure of the known form III of tolbutamide instead of the anticipated co-crystals. A novel form V of tolbutamide was crystallized when a trace of conc. HNO3 was added in MeOH solvent.

Graphical abstract: Novel form V of tolbutamide and a high Z′ crystal structure of form III

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Article information

DOI
https://doi.org/10.1039/C0CE00073F
Article type
Communication
Submitted
09 Apr 2010
Accepted
10 Oct 2010
First published
28 Oct 2010

CrystEngComm, 2011,13, 47-51

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Novel form V of tolbutamide and a high Z′ crystal structure of form III

N. K. Nath and A. Nangia, CrystEngComm, 2011, 13, 47 DOI: 10.1039/C0CE00073F

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