Issue 1, 2011

High-resolution solid-state 13C μMAS NMR with long coherence life times

Abstract

Longer coherence life times (i.e. smaller homogeneous linewidths) can be achieved for carbon resonances which are strongly coupled to protons with high rf field heteronuclear decoupling in micro magic angle spinning NMR. Better proton decoupling enhances the sensitivity and resolution of two-dimensional through-bond correlation experiments for mass-limited samples with uniform carbon labeling.

Graphical abstract: High-resolution solid-state 13C μMAS NMR with long coherence life times

Supplementary files

Article information

Article type
Communication
Submitted
24 Sep 2010
Accepted
18 Oct 2010
First published
12 Nov 2010

Phys. Chem. Chem. Phys., 2011,13, 104-106

High-resolution solid-state 13C μMAS NMR with long coherence life times

S. K. Vasa, H. Janssen, E. R. H. Van Eck and A. P. M. Kentgens, Phys. Chem. Chem. Phys., 2011, 13, 104 DOI: 10.1039/C0CP01929A

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