BOP-mediated one-pot synthesis of C5-symmetric macrocyclic pyridone pentamers

Zhiyun Du; Changliang Ren; Ruijuan Ye; Jie Shen; Victor Maurizot; Yujin Lu; Jian Wang; Huaqiang Zeng

doi:10.1039/C1CC14377H

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BOP-mediated one-pot synthesis of C₅-symmetric macrocyclic pyridone pentamers†

Zhiyun Du,^ab Changliang Ren,^b Ruijuan Ye,^b Jie Shen,^b Victor Maurizot,^c Yujin Lu,^a Jian Wang^b and Huaqiang Zeng*^b

Author affiliations

* Corresponding authors

^a Faculty of Light Industry and Chemical Engineering, Guang Dong University of Technology, Guang Dong, China

^b Department of Chemistry, National University of Singapore, 3 Science Drive 3, Singapore
E-mail: chmzh@nus.edu.sg
Tel: +65-6516-2683

^c CNAB–UMR5084, Université de Bordeaux, UMR CNRS 5248, Institute Européen de Chimie et Biologie (IECB), 2 rue Robert Escarpit, 33607 Pessac Cedex, France

Abstract

We report here, for the first time, the BOP-mediated one-pot macrocyclization that is facilitated and guided by internally placed intramolecular H-bonds to allow for the highly selective formation of five-residue cation-binding macrocycles.

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Article information

DOI: https://doi.org/10.1039/C1CC14377H
Article type: Communication
Submitted: 20 Jul 2011
Accepted: 26 Sep 2011
First published: 21 Oct 2011

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Chem. Commun., 2011,47, 12488-12490

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BOP-mediated one-pot synthesis of C₅-symmetric macrocyclic pyridone pentamers

Z. Du, C. Ren, R. Ye, J. Shen, V. Maurizot, Y. Lu, J. Wang and H. Zeng, Chem. Commun., 2011, 47, 12488 DOI: 10.1039/C1CC14377H

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