TiCl3·THF is reduced by metallic magnesium in tetrahydrofuran (THF) under argon or nitrogen to a product which reductively removes halogen atoms from both sp3 and sp3 hybridised organic halides.
S. Tyrlik and I. Wołochowicz, J. Chem. Soc., Chem. Commun., 1975, 781 DOI: 10.1039/C39750000781
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