The compounds Cu4[SC(NH2)2]6(NO3)4·4H2O and Cu4[SC(NH2)2]9(NO3)4·4H2O have been prepared, their structures determined, and are shown to contain a central Cu4S6 core with four trigonal planar Cu atoms in the former, but only one trigonal planar Cu in the latter.
E. H. Griffith, G. W. Hunt and E. L. Amma, J. Chem. Soc., Chem. Commun., 1976, 432 DOI: 10.1039/C39760000432
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