The reaction of [Os6(CO)18] with [Os3(CO)11H]– gives the anion [HOs3(CO)10·O2C·Os6(CO)17]– which has been fully characterized by a single crystal X-ray diffraction study on the [(Ph3P)2N]+ salt.
C. R. Eady, J. J. Guy, B. F. G. Johnson, J. Lewis, M. C. Malatesta and G. M. Sheldrick, J. Chem. Soc., Chem. Commun., 1976, 602 DOI: 10.1039/C39760000602
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