Hydrogenolysis of hexamethyltungsten in the presence of PPhPri2 affords [WH6(PPhPri2)3], which is shown by 31P n.m.r. spectroscopy and X-ray diffraction to have approximate C2v symmetry in the solid and in solution.
D. Gregson, J. A. K. Howard, J. N. Nicholls, J. L. Spencer and D. G. Turner, J. Chem. Soc., Chem. Commun., 1980, 572 DOI: 10.1039/C39800000572
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