Reaction of [HOs3(CO)11]– with [Fe2(CO)9] in refluxing tetrahydrofuran leads to the isolation of [HOs4(CO)13]–, which has been shown by spectroscopic and X-ray crystallographic techniques to contain an Os4 tetrahedron, one edge of which is bridged by a CO ligand.
P. A. Dawson, B. F. G. Johnson, J. Lewis, D. A. Kaner and P. R. Raithby, J. Chem. Soc., Chem. Commun., 1980, 961 DOI: 10.1039/C39800000961
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