Reaction of Ph3P+SRClO4–, prepared electrochemically from RSSR and Ph3P, with thiols in n-hexane at room temperature gave unsymmetrical disulphides in excellent yields with recovery of Ph3P.
M. Masui, Y. Mizuki, K. Sakai, C. Ueda and H. Ohmori, J. Chem. Soc., Chem. Commun., 1984, 843 DOI: 10.1039/C39840000843
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