27 Al Magic angle spining n.m.r. and i.r. spectroscopy show that introduction of 4-and 6-co-ordinated aluminium occurs during treatment of highly-siliceous ZSM-5/silicalite with AlCl3 vapour at elevated temperatures.
M. W. Anderson, J. Klinowski and L. Xinsheng, J. Chem. Soc., Chem. Commun., 1984, 1596 DOI: 10.1039/C39840001596
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