[IrH5(PCy3)2](Cy = Cyclohexyl) is shown by n.m.r. evidence, including T1 measurements, to undergo protonation to give the title complex, a bis(dihydrogen) dihydride, the first example of a non-classical polyhydride complex.
R. H. Crabtree and M. Lavin, J. Chem. Soc., Chem. Commun., 1985, 1661 DOI: 10.1039/C39850001661
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