X-Ray investigations of single crystals of bismuth(III) 2,2-dimethylpropanoate (pivalate), obtained by sublimation in vacuo, reveal its structure to consist of isolated tetrameric units [Bi(O2CCMe3)3]4; each of the twelve crystallographically inequivalent Bi atoms has practically the same coordination environment of nine O atoms at distances of 2.24–3.27 Å.
S. I. Troyanov and A. P. Pisarevsky, J. Chem. Soc., Chem. Commun., 1993, 335 DOI: 10.1039/C39930000335
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