Single-crystal X-ray diffraction studies of the oligomers m-deciphenyl and m-undeciphenyl, isolated chromatographically from low molecular mass poly(m-phenylene), reveal disordered but unequivocally helical chain-structures, from which the crystal and molecular structure of poly(m-phenylene) can be directly inferred.
D. J. Williams, H. M. Colquhoun and C. A. O'Mahoney, J. Chem. Soc., Chem. Commun., 1994, 1643 DOI: 10.1039/C39940001643
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