Issue 9, 2014
From the journal:

Chemical Communications

One-pot synthesis of d-glucosamine and chitobiosyl building blocks catalyzed by triflic acid on molecular sieves†

Guillaume Despras,a   Dominique Urban,a   Boris Vauzeillesab  and  Jean-Marie Beau*ab  

* Corresponding authors

a Université Paris-Sud and CNRS, Laboratoire de Synthèse de Biomolécules, Institut de Chimie Moléculaire et des Matériaux d'Orsay, F-91405 Orsay, France
E-mail: jean-marie.beau@u-psud.fr
Fax: +33 1 69 85 37 15
Tel: +33 1 69 15 79 60

b Centre de Recherche de Gif, Institut de Chimie des Substances Naturelles du CNRS, Avenue de la Terrasse, F-91198 Gif-sur-Yvette, France

Abstract

Combining triflic acid-catalyzed acetalation, benzylation, reductive ring opening of benzylidene acetal and glycosylation in one-pot transformations leads to a wide range of D-glucosamine building blocks for assembling oligomers.

Graphical abstract: One-pot synthesis of d-glucosamine and chitobiosyl building blocks catalyzed by triflic acid on molecular sieves

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Article information

DOI
https://doi.org/10.1039/C3CC48078J
Article type
Communication
Submitted
21 Oct 2013
Accepted
15 Nov 2013
First published
15 Nov 2013

Chem. Commun., 2014,50, 1067-1069

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One-pot synthesis of D-glucosamine and chitobiosyl building blocks catalyzed by triflic acid on molecular sieves

G. Despras, D. Urban, B. Vauzeilles and J. Beau, Chem. Commun., 2014, 50, 1067 DOI: 10.1039/C3CC48078J

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