SCHEDULED MAINTENANCE
Readily prepared 2-arylacetic anhydrides act as convenient ammonium enolate precursors in isothiourea (HBTM-2.1)-mediated catalytic asymmetric intermolecular Michael addition–lactonisation processes, giving diverse synthetic building blocks in good yield with high diastereo- and enantiocontrol (up to 98 : 2 dr and >99% ee).
L. C. Morrill, L. A. Ledingham, J. Couturier, J. Bickel, A. D. Harper, C. Fallan and A. D. Smith, Org. Biomol. Chem., 2014, 12, 624 DOI: 10.1039/C3OB41869C
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