Issue 6, 2015
From the journal:

Analyst

En route to traceable reference standards for surface group quantifications by XPS, NMR and fluorescence spectroscopy†

Andreas Hennig,*ab   Paul M. Dietrich,*a   Felix Hemmann,a   Thomas Thiele,c   Heike Borcherding,c   Angelika Hoffmann,a   Uwe Schedler,c   Christian Jäger,a   Ute Resch-Genger*a  and  Wolfgang E. S. Ungera  

* Corresponding authors

a BAM Federal Institute for Materials Research and Testing, Richard-Willstaetter-Strasse 11, 12203 Berlin, Germany
E-mail: paul.dietrich@bam.de, ute.resch@bam.de

b Jacobs University Bremen, School of Engineering and Science, Campus Ring 1, 28759 Bremen, Germany
E-mail: a.hennig@jacobs-university.de

c PolyAn GmbH, Rudolf-Baschant-Strasse 2, 13086 Berlin, Germany

Abstract

The fluorine content of polymer particles labelled with 2,2,2-trifluoroethylamine was reliably quantified with overlapping sensitivity ranges by XPS and solid-state NMR. This provides a first step towards reference materials for the metrological traceability of surface group quantifications. The extension of this concept to fluorescence spectroscopy is illustrated.

Graphical abstract: En route to traceable reference standards for surface group quantifications by XPS, NMR and fluorescence spectroscopy

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Article information

DOI
https://doi.org/10.1039/C4AN02248C
Article type
Communication
Submitted
08 Dec 2014
Accepted
28 Jan 2015
First published
28 Jan 2015
This article is Open Access
Creative Commons BY license

Analyst, 2015,140, 1804-1808

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En route to traceable reference standards for surface group quantifications by XPS, NMR and fluorescence spectroscopy

A. Hennig, P. M. Dietrich, F. Hemmann, T. Thiele, H. Borcherding, A. Hoffmann, U. Schedler, C. Jäger, U. Resch-Genger and W. E. S. Unger, Analyst, 2015, 140, 1804 DOI: 10.1039/C4AN02248C

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