Issue 92, 2014
From the journal:

Chemical Communications

A facile single crystal to single crystal transition with significant structural contraction on desolvation†

Jane V. Knichal,a   William J. Gee,a   Andrew D. Burrows,*a   Paul R. Raithby,*a   Simon J. Teatb  and  Chick C. Wilson*a  

* Corresponding authors

a Department of Chemistry, University of Bath, Claverton Down, Bath BA2 7AY, UK
E-mail: C.C.Wilson@bath.ac.uk
Web: http://www.metastable-materials.org.uk/

b Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, CA 947240, USA

Abstract

5-Ethynyl-1,3-benzenedicarboxylic acid (H2ebdc) reacted with lead(II) acetate trihydrate yields a 1D ladder network, [Pb(ebdc)(MeOH)]2·H2O (1). Removing crystals of 1 from the mother liquor results in a facile single crystal to single crystal transition, yielding 2D [Pb(ebdc)] net (2) with a change in space group from I2/a to P[1 with combining macron].

Graphical abstract: A facile single crystal to single crystal transition with significant structural contraction on desolvation

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Article information

DOI
https://doi.org/10.1039/C4CC06587E
Article type
Communication
Submitted
21 Aug 2014
Accepted
26 Sep 2014
First published
01 Oct 2014
This article is Open Access
Creative Commons BY license

Chem. Commun., 2014,50, 14436-14439

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A facile single crystal to single crystal transition with significant structural contraction on desolvation

J. V. Knichal, W. J. Gee, A. D. Burrows, P. R. Raithby, S. J. Teat and C. C. Wilson, Chem. Commun., 2014, 50, 14436 DOI: 10.1039/C4CC06587E

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