Issue 86, 2016
From the journal:

Chemical Communications

Rapid and safe ASAP acquisition with EXACT NMR†

I. E. Ndukwe,a   A. Shchukina,bc   K. Kazimierczukb  and  C. P. Butts*a  

* Corresponding authors

a School of Chemistry, University of Bristol, Cantocks Close, Bristol, UK
E-mail: Craig.Butts@bris.ac.uk

b Centre of New Technologies, University of Warsaw, Banacha 2C, Warszawa, Poland

c Institute for Spectroscopy, Russian Academy of Sciences, Fizicheskaya 5, Moscow, Troitsk, Russia

Abstract

The dangerously high power levels required for fast ASAP-HSQC and ASAP-HMQC experiments are mitigated by employing EXACT NMR. The utility of this technique is demonstrated by application of the EXACT ASAP-HSQC to chemical reaction monitoring, accelerating data acquisition by up to 2 orders of magnitude – providing evidence of it's value in fast quantitative NMR processes.

Graphical abstract: Rapid and safe ASAP acquisition with EXACT NMR

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Article information

DOI
https://doi.org/10.1039/C6CC07140F
Article type
Communication
Submitted
31 Aug 2016
Accepted
06 Oct 2016
First published
06 Oct 2016

Chem. Commun., 2016,52, 12769-12772

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Rapid and safe ASAP acquisition with EXACT NMR

I. E. Ndukwe, A. Shchukina, K. Kazimierczuk and C. P. Butts, Chem. Commun., 2016, 52, 12769 DOI: 10.1039/C6CC07140F

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