An integrated total neutron scattering – NMR approach for the study of heterogeneous catalysis

Markus Leutzsch; Marta Falkowska; Terri-Louise Hughes; Andrew J. Sederman; Lynn F. Gladden; Michael D. Mantle; Tristan G. A. Youngs; Daniel Bowron; Haresh Manyar; Christopher Hardacre

doi:10.1039/C8CC04740E

An integrated total neutron scattering – NMR approach for the study of heterogeneous catalysis†

Markus Leutzsch,

‡^a Marta Falkowska,

‡^b Terri-Louise Hughes,

‡^b Andrew J. Sederman,

^a Lynn F. Gladden,

^a Michael D. Mantle,

*^a Tristan G. A. Youngs,

^c Daniel Bowron,

^c Haresh Manyar

^d and Christopher Hardacre

*^b

Author affiliations

* Corresponding authors

^a Department of Chemical Engineering and Biotechnology, Philippa Fawcett Drive, University of Cambridge, Cambridge, UK
E-mail: mdm20@cam.ac.uk

^b School of Chemical Engineering and Analytical Science, The University of Manchester, Manchester, UK
E-mail: c.hardacre@manchester.ac.uk

^c STFC ISIS Facility, Rutherford Appleton Laboratory Chilton, Didcot, Oxon, UK

^d School of Chemistry and Chemical Engineering, Queen's University Belfast, Belfast, UK

Abstract

Nuclear magnetic resonance (NMR) and total neutron scattering techniques are established methods for the characterisation of liquid phases in confined pore spaces during chemical reactions. Herein, we describe the first combined total neutron scattering – NMR setup as a probe for the catalytic heterogeneous reduction of benzene-d₆ with D₂ in 3 wt% Pt/MCM-41.

Chemical Communications

An integrated total neutron scattering – NMR approach for the study of heterogeneous catalysis†

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An integrated total neutron scattering – NMR approach for the study of heterogeneous catalysis

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