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But-1-enyl(methyl)maleic anhydride (4) has been synthesised and shown to act as an efficient (55% incorporation) precursor of the cyclononadienes, glauconic and glaucanic acids, in Penicillium purpurogenum. Base-catalysed dimerisation of compound (4) yields 5% of an epimer of glaucanic acid.
R. K. Huff, C. E. Moppett and J. K. Sutherland, J. Chem. Soc., Perkin Trans. 1, 1972, 2584 DOI: 10.1039/P19720002584
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