SCHEDULED MAINTENANCE
Reaction conditions for electroreductive conversion of 1-halogenopentane into hexanal using [Fe(CO)5] have been investigated in detail. The use of acetonitrile as solvent containing tetraalkylammonium halides or toluene-p-sulfonate and a divided cell gave good results. Under the conditions, the best results were obtained with the bromide as starting halide.
K. Yoshida, M. Kobayashi and S. Amano, J. Chem. Soc., Perkin Trans. 1, 1992, 1127 DOI: 10.1039/P19920001127
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