The oxidative coupling of methyl sinapate with H2O2/horse radish peroxidase at pH 4 in the presence of methanol gives dimeric spiro structures of a novel type. The crystal structures of two diastereoisomers have been determined. The coupling reaction shows some threo selectivity.
H. Setälä, A. Pajunen, I. Kilpeläinen and G. Brunow, J. Chem. Soc., Perkin Trans. 1, 1994, 1163 DOI: 10.1039/P19940001163
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