Issue 9, 2007
From the journal:

CrystEngComm

Solvent inclusion in the structural voids of form II carbamazepine: single-crystal X-ray diffraction, NMR spectroscopy and Hirshfeld surface analysis†‡

Francesca P. A. Fabbiani,*a   Lindsay T. Byrne,a   Joshua J. McKinnona  and  Mark A. Spackman*a  

* Corresponding authors

a School of Biomedical, Biomolecular & Chemical Sciences, University of Western Australia, Crawley, Australia
E-mail: francescapa@gmail.com, mas@cyllene.uwa.edu.au
Fax: +61 8 6488 1005
Tel: +61 8 6488 3140

Abstract

Single-crystal X-ray diffraction and solution 1H NMR spectroscopy, in conjunction with Hirshfeld surface analysis, give evidence of solvent inclusion in the trigonal polymorph of carbamazepine, which in the unsolvated form is characterised by the presence of large structural voids.

Graphical abstract: Solvent inclusion in the structural voids of form II carbamazepine: single-crystal X-ray diffraction, NMR spectroscopy and Hirshfeld surface analysis

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Article information

DOI
https://doi.org/10.1039/B708303N
Article type
Communication
Submitted
31 May 2007
Accepted
06 Jun 2007
First published
25 Jun 2007

CrystEngComm, 2007,9, 728-731

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Solvent inclusion in the structural voids of form II carbamazepine: single-crystal X-ray diffraction, NMR spectroscopy and Hirshfeld surface analysis

F. P. A. Fabbiani, L. T. Byrne, J. J. McKinnon and M. A. Spackman, CrystEngComm, 2007, 9, 728 DOI: 10.1039/B708303N

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