Here, accompanied by in situ Raman monitoring, we adapt the aza-Michael addition for the formation of the C–N bond under mechanochemical conditions, enabling solvent- and catalyst-free synthesis and facile preparation of compounds that are challenging to obtain in solution.
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L. Vugrin, A. Bjelopetrović and I. Halasz, RSC Mechanochem., 2025, 2, 184 DOI: 10.1039/D4MR00133H
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