Issue 11, 2002
From the journal:

Chemical Communications

A one-step synthesis of fused pentathiepins†

Lidia S. Konstantinova,a   Oleg A. Rakitina  and  Charles W. Reesb  

a N. D. Zelinsky Institute of Organic Chemistry, Academy of Sciences, Leninsky Prospect, 47, 119991 Moscow, Russia
E-mail: orakitin@ioc.ac.ru

b Department of Chemistry, Imperial College of Science, Technology and Medicine, London, UK
E-mail: c.rees@ic.ac.uk

Abstract

Treatment of nucleophilic heterocycles like pyrroles and thiophene, and their tetrahydro derivatives, with S2Cl2 and a base in chloroform at room temperature provides a simple one-pot synthesis of heterocyclic fused mono and bis pentathiepins such as 2, 3, 4, 5, 9, and 11.

Graphical abstract: A one-step synthesis of fused pentathiepins

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Article information

DOI
https://doi.org/10.1039/B203349F
Article type
Communication
Submitted
05 Apr 2002
Accepted
22 Apr 2002
First published
02 May 2002

Chem. Commun., 2002, 1204-1205

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A one-step synthesis of fused pentathiepins

L. S. Konstantinova, O. A. Rakitin and C. W. Rees, Chem. Commun., 2002, 1204 DOI: 10.1039/B203349F

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