Issue 5, 2000
From the journal:

Journal of Materials Chemistry

Xiqu Wang,a   Lumei Liu,a   Heidi Cheng,a   Kent Rossa  and  Allan J. Jacobson*a  

* Corresponding authors

a Department of Chemistry, University of Houston, Houston, Texas, USA
E-mail: ajjacob@uh.edu

Abstract

The new niobium phosphates [H3N(CH2)2NH3]NbFeOF(PO4)2(H2O)2 and [H3N(CH2)2NH3]NbCoOF(PO4)2(H2O)2 have been synthesized in single crystal form by hydrothermal reactions at 165 °C. The new phase [H3N(CH2)2NH3]Ti(Fe0.9Cr0.1)(F1.3O0.7)(H0.3PO4)2(H2O)2 has been obtained by hydrothermal electrocrystallization at 170 °C. The crystal structures have been refined from X-ray diffraction data. They are structurally similar to the known layered iron phosphate [H3N(CH2)2NH2][Fe2F2(HPO4)2(H2O)2] designated as ULM-10 and the mineral curetonite.

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Article information

DOI
https://doi.org/10.1039/A909193I
Article type
Paper
Submitted
22 Nov 1999
Accepted
08 Feb 2000
First published
13 Apr 2000

J. Mater. Chem., 2000,10, 1203-1208

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Synthesis and crystal structures of [H3N(CH2)2NH3]NbMOF(PO4)2(H2O)2, M = Fe,Co and [H3N(CH2)2NH3]Ti(Fe0.9Cr0.1)(F1.3O0.7)(H0.3PO4)2(H2O)2

X. Wang, L. Liu, H. Cheng, K. Ross and A. J. Jacobson, J. Mater. Chem., 2000, 10, 1203 DOI: 10.1039/A909193I

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